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Research Services

INSTRUMENTAL ANALYSIS
Staff:
RESEARCH SERVICES - Staff

Service Manager
Miguel Ángel Fernández Recio
CSIC R&D&I Technician
941894980 | mirecio@icvv.es

PTA Technitian
Cristrina Moreta Sanchez
CSIC Higher graduate
941894980 | cristina.moreta@icvv.es

Support technitian
Roxana Mihalache
CSIC Internship Technician
941894980 | roxana.mihalache@icvv.es

Funciones principales

- Analytical services to ICVV and external researchers.

- Advice on the different available analytical techniques.

- Centralized laboratory and analytical equipment maintenance.

- Cryogenic and compressed gases management.

- Dangerous wastes management.

- Purified water management.
 

Equipment:

Currently available equipment:

Equipamiento

UHPLC-DAD-ESI/APCI-MS/MS

Shimadzu Nexera UHPLC (ultra high pressure liquid chromatography) with photodiode array detector (DAD), coupled to an atmospheric pressure ionization source (ESI and APCI) ABSciex 3200QTRAP® triple quadrupole/ion trap mass spectrometer.

UHPLC-DAD
Shimadzu Nexera UHPLC (ultra high pressure liquid chromatography) with photodiode array detector (DAD).
HPLC-FD-LSD
Shimadzu Prominence UFLC (ultra fast liquid chromatography) with fluorescence detector (FD), refraction index detector (RID) and evaporative light scattering detector (ELSD).
GC-MS:
Agilent 7890 gas chromatograph, with SSL and PTV injectors, including a thermal desorption system, coupled to an Agilent 7000C triple quadrupole mass spectrometer Gerstel MPS automatized sample injection system (SPME, liquids, Headspace, Twister).
SemiPrep-HPLC:
Gilson semipreparative HPLC chromatograph with photodiode array detector (DAD) and Gilson GX271 automatized fraction injection/collection auto sampler.
SPE:
Gilson GX271 automatized solid phase extraction system.
Available services

- Qualitative analysis of complex mixtures by means of chromatographic separation (LC and GC). Detectors: DAD and mass spectrometer (MS, MS2 and MS3).

- Offered provisions:

  • • Polyphenol LC analysis (anthocyanins, phenolic acids, flavonols, flavanols, stilbenes, lignans)
  • • Aminoacids and amines LC analysis
  • • Volatile compounds  GC analysis (acids, alcohols, aromatic compounds)
  • • Short chain fatty acids (SCFA) GC analysis

- Handling of different matrixes: vegetable samples (fermented product, juice, pulp, skin, seed), biological samples (urine, faeces)
- Development of chromatographic methods.
- Technical advice and training of the ICVV internal users at GC-MS, SemiPrep-HPLC, SPE, UHPLC-DAD and HPLC-FD-RID-LSD.
- The comprehensive provision catalogue and fees for ICVV and CSIC institutes internal users are located in CSIC institutes personnel Intranet (Catálogo de prestaciones del CSIC)
- The available provisions and fees for external users will be provided by contacting with Instrumental Analysis Service (on-line Catalogue on build)
- On-line analysis application form (on build).